Abstract
Gas chromatography chemical ionization mass spectrometry has been found to possess advantages over gas chromatography electron impact mass spectrometry for the structural elucidation of glucosinolates (mustard oil glycosides), separated as the volatile per-trimethylsilyldesulpho derivates. The method has been applied to both mixtures of standard glucosinolates and also to extracts of plant tissue. The technique demonstrates the versatility of mass spectrometry in glucosinolate identification.
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