Abstract
An alkene in which the double bond is flanked by hydrocarbon asymmetric centers exists as a pair of diastereomers that often can be resolved by gas chromatography. The resolution of a series of such diastereomers on a bonded non-polar column is described. The elution order of the diastereomers, the variation of separation factors with the distance between the asymmetric centers, and the potential for using this information to analyze natural products for configuration and configurational purity are discussed.
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