Abstract
Gallium(III) and indium(III) complexes of cross-bridged cyclam and cyclen tetraaza macrocyclic ligands have been prepared and structurally characterized. In the crystalline state, both the GaCl 3 (cross-bridged cyclam) and InBr 3 (cross-bridged cyclen) complexes feature hexacoordinate cations in cis-folded tetradentate ligand clefts with ancillary cis-dihalides. These represent the first well-characterized gallium and indium halide complexes of tetraazamacrocycles.
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