Abstract
AbstractRadiation‐induced polymerization of 2,3‐dichlorobutadiene in deoxycholic acid canal complexes was studied under various reaction conditions. The rate of polymerization was found to increase with raising reaction temperature and increasing irradiation dose. The apparent activation energy was obtained as 14.3 kJ/mol in the temperature range between −23° and 50°C. Results from differential thermal analysis and infrared spectroscopy explain the gradual change of the monomer into polymer within canal complexes.
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