Abstract
The nucleation and growth of nanoscale precipitates in a new class of high-strength, multicomponent, ferritic steels has been studied with complementary state-of-the-art microstructural characterization techniques of atom probe tomography for individual embryos and precipitates and small-angle neutron scattering for their statistical averages. Both techniques revealed a bimodal size distribution, with subnanometer embryos, and nanoscale precipitates. The embryos, which have a radius of \ensuremath{\sim}0.4 nm, are enriched in Cu and served as preferential sites for nucleation. The critical radius for nucleation was determined to be \ensuremath{\sim}0.7 nm. Subsequent growth of the precipitates is dictated by volumetric diffusion, as predicted by the Lifshitz--Slyozov--Wagner theory.
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