Fracture Toughness of Silicon Nitride Measured by the Surface Crack in Flexure (SCF) Test Method

Abstract

The surface crack in flexure (SCF) is a method for the evaluation of the fracture toughness of advanced ceramics. Conventionally is practiced by using a Knoop indenter to make a very small pre-crack. Removal on indent and the plastically deformed zone is required before the fracture test. The purpose of this removal is to eliminate residual stresses under the Knoop impression and to obtain a semi elliptical pre-crack shape. In this work fracture toughness values by the SCF method are compared with those measured using the SEVNB (single edge V-notched beam) method. The material chosen for this purpose was gas pressured sintered silicon nitride (Si3N4) containing 3wt. % Al2O3 and 3 wt. % Y2O3 (SL200B, Ceram Tec, Plochingen, Germany). The varied parameters the amount of material removed from the surface. Short specimens with size 3 x 4 x >25 mm were prepared for this purpose. The fracture toughness of specimens with a surface removal in the range suggested from ASTM C 1421 were found to agree with the results obtained from SEVNB. A surface removal below the recommendation resulted in low values of fracture toughness. Increasing the amount of surface removal moderately was found to still fit with results obtained from SEVNB. Surface removal of much more from the recommended amount leads to failure from natural flaws.