Fracture toughness and hardness evaluation of three pressable all-ceramic dental materials

Abstract

Objectives. This study evaluates the fracture toughness and hardness of three pressable all-ceramic materials: IPS-Empress, Empress 2 and an experimental ceramic material. Methods. Fifteen discs and 15 bars per material were prepared. Fracture toughness was measured with two different techniques: indentation fracture and indentation strength. During the indentation fracture tests the hardness of each material was also measured. Statistical significance among groups of population was studied using one-way Anova and Tukey's multiple comparison tests. Results. Fracture toughness results using the indentation strength technique (with three-point bending and biaxial flexure tests) were: IPS-Empress (1.39 (SD 0.3) and 1.32 (SD 0.3)); Empress 2 (3.14 (SD 0.5) and 2.50 (SD 0.3)) MPa· m 1/2; and the experimental ceramic (3.32 (SD 0.6) and 2.43 (SD 0.3)) MPa· m 1/2. The indentation fracture technique generated orthogonal cracks of different lengths for Empress 2 and the experimental ceramic, whether perpendicular or parallel to the lithium disilicate elongated crystals. Thus, two values were reported: Empress 2 (1.5 (SD 0.2) and 1.16 (SD 0.2)) MPa· am 1/2 and the experimental ceramic (1.67 (SD 0.3) and 1.15 (SD 0.15)) MPa· m 1/2. The IPS-Empress indentation fracture result was 1.26 (SD 0.1). The hardness results were: 6.6, 5.3 and 5.5 GPa for IPS-Empress, Empress 2 and the experimental ceramic, respectively. Conclusions. No significant differences in fracture toughness and hardness results were found between Empress 2 and the experimental ceramic ( P>0.05 ANOVA). Both materials exhibited fracture toughness anisotropy following pressing. They demonstrated improved fracture toughness and reduced hardness compared with IPS-Empress P<0.05(ANOVA), which should be beneficial for clinical applications.