Abstract

Studying complex pore structures and fractal characteristics of gas shale provides significant guidance for clarifying the mechanism of shale gas accumulation and realizing its efficient development. In this paper, 12 samples of Taiyuan Formation shale are used as the research object, and the fractal theory is combined with mercury intrusion porosimetry and N2 adsorption technology to innovatively solve the problem of splicing point selection, which can reveal the full-scale pore size distribution of shale. The results demonstrate that the most common types of pores in the chosen samples are pores between or within clay minerals, micropores and mesopores inside organic matter, and microfractures, based on scanning electron microscopy imagery analyses. The pores of shale samples have fractal geometries. The fractal dimension DM1 values in the mercury intrusion porosimetry experiments range from 2.3060 to 2.6528. Two fractal dimensions, DN1 and DN2, may be obtained using the Frenkel-Halsey-Hill fractal method. DN1 values vary from 2.4780 to 2.6387, whereas DN2 values range from 2.5239 to 2.7388. Most macropores in shale samples have a size range of about 0.2 mm, with a wide pore size distribution, and the largest peak of the micro-mesopore volume is generally about 50 nm. The fractal dimension correlates positively with the corresponding pore volume, although the correlation between volume and composition is weak. The relatively strong correlation between fractals and the basic compositions of shale proves the fractal theory’s relevance in defining pore inhomogeneity. This study would contribute to the development of a fractal perspective-based method for pore splicing while also expanding our understanding of pore morphology and structure in transitional shale.

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