Abstract
Both square planar and tetrahedral isomers of the four-coordinate complex [Co(Bc(tBu))2] with a bis(3-tert-butylimidazol-2-ylidene)borate ligand (Bc(tBu)) have been isolated while only a tetrahedral configuration was found for the Fe(ii) analogue [Fe(Bc(tBu))2]. Novel co-crystals containing both isomers of [Co(Bc(tBu))2] have been obtained from recrystallization.
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