Abstract
The compound [ArZn(OH)] 4 (Ar = 2,4,6-(CF 3) 3C 6H 2), formed by aggregation of the hydrolysis product of ArZnCl, has a cubane-like structure at 120 K; this is the first structurally characterised example of such a zinc(II) derivative with a simple aromatic group on Zn, and with the bridges formed by –OH rather than –OR groups. It crystallises as a hemisolvate in the triclinic system ( P 1 ¯ ) , with a single molecule in the asymmetric unit, together with one CHCl 3 (or CDCl 3) molecule per two molecules of the tetramer.
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