Abstract

The formation of stacking faults and dislocations in individual austenite (fcc) grains embedded in a polycrystalline bulk Fe-18Cr-10.5Ni (wt.%) steel was investigated by non-destructive high-energy diffraction microscopy (HEDM) and line profile analysis. The broadening and position of intensity, diffracted from individual grains, were followed during in situ tensile loading up to 0.09 strain. Furthermore, the predominant deformation mechanism of the individual grains as a function of grain orientation was investigated, and the formation of stacking faults was quantified. Grains oriented with [100] along the tensile axis form dislocations at low strains, whilst at higher strains, the formation of stacking faults becomes the dominant deformation mechanism. In contrast, grains oriented with [111] along the tensile axis deform mainly through the formation and slip of dislocations at all strain states. However, the present study also reveals that grain orientation is not sufficient to predict the deformation characteristics of single grains in polycrystalline bulk materials. This is witnessed specifically within one grain oriented with [111] along the tensile axis that deforms through the generation of stacking faults. The reason for this behavior is due to other grain-specific parameters, such as size and local neighborhood.

Highlights

  • Austenitic stainless steels are of considerable engineering importance due to their excellent corrosion resistance and mechanical properties [1,2]

  • Dislocations and stacking faults have been investigated in individual grains embedded within a polycrystalline bulk austenitic stainless steel

  • In situ X-ray line profile analysis was successfully applied to six individual grains with different orientations with respect to the external load

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Summary

Introduction

Austenitic stainless steels are of considerable engineering importance due to their excellent corrosion resistance and mechanical properties [1,2]. In these steels, it is known that the stacking fault energy (γSF ) can be used to predict the predominantly active deformation mechanism controlling the material’s mechanical properties. Austenitic stainless steels with a low γSF are known to form large stacking faults and undergo deformation-induced martensitic phase transformation responsible for the well-known transformation-induced plasticity (TRIP). The predominantly active deformation mechanism varies across the bulk [8,9,10] and it is necessary to consider all the mentioned parameters to predict the active deformation mechanism on the local scale

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