Abstract
Single crystals of the ternary palladates SrPd3O4 and CaPd3O4 have been grown out of a potassium hydroxide flux. Small cubic crystals can be readily isolated from the soluble flux matrix and characterized by SEM and single-crystal X-ray diffraction. Both SrPd3O4 and CaPd3O4 crystallize with the NaPt3O4 structure and feature square planar coordination of palladium atoms. SrPd3O4 and CaPd3O4 crystallize in space group Pm3̄n (no. 223) with a=5.8120(7)Å, V=196.33(4)Å3, Z=2, R1=0.042, wR2=0.091 and a=5.7356(3)Å, V=188.68(2)Å3, Z=2, R1=0.034, wR2=0.076, respectively.
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