Abstract

A reactor has been designed and built to handle anhydrous HF and SF 4 safely for routineuse in organic synthesis. The system described is completely contained and remotelyoperated so as to minimize any possible exposure to these dangerous materials. Furthermore,it features controls that allow the experimentalist to accurately add HF andSF 4, monitor the reaction progress and sample ff necessary, as well as allowing flexibilityin the work-up of the reaction.

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