Abstract
Several Lewis acid–base adducts R 3Al←SbR′ 3 (R′=Et, R=Me ( 1), Et ( 2), t-Bu ( 3); R′= n-Pr, R=Me ( 4), Et ( 5), t-Bu ( 6); R′= i-Pr, R=Me ( 7), Et ( 8), t-Bu ( 9); R′= sec-Bu, R=Me ( 10), Et ( 11), t-Bu ( 12); R′= t-Bu, R=Me ( 13), Et ( 14), t-Bu ( 15)) were obtained by reaction of aluminum trialkyls R 3Al and the corresponding antimony trialkyls R′ 3Sb. For the first time, solid state structures of all-alkyl substituted Al–Sb adducts ( 3, 9, 13, 14) were determined by single crystal X-ray analysis.
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