Abstract
This article presents a field-emission electron gun intended for use in a MEMS (microelectromechanical system) electron microscope. Its fabrication process follows the technology of a miniature device under development built from silicon electrodes and glass spacers. The electron gun contains a silicon cathode with a single very sharp protrusion and a bundle of disordered CNTs deposited on its end (called a sharp silicon/CNT cathode). It was tested in diode and triode configurations. For the diode configuration, a low threshold voltage <1000 V and a high emission current that reached 90 µA were obtained. After 30 min of operation at 900 V, the emission current decreased to 1.6 µA and was stable for at least 40 min, with RMS fluctuation in the anode current lower than 10%. The electron beam spot of the source was observed on the phosphor screen. In the diode configuration, the spot size was the same as the emission area (~10 µm), which is a satisfactory result. In the triode configuration, an extraction electrode (gate) control function was reported. The gate limited the emission current and elongated the lifetime of the gun when the current limit was set. Moreover, the electron beam current fluctuations at the anode could be reduced to ~1% by using a feedback loop circuit that controls the gate voltage, regulating the anode current. The developed sharp silicon/CNT cathodes were used to test the MEMS electron source demonstrator, a key component of the MEMS electron microscope, operating under atmospheric pressure conditions. Cathodoluminescence of the phosphor layer (ZnS:Ag) deposited on the thin silicon nitride membrane (anode) was observed.
Highlights
The electron beam parameters of an electron microscope, i.e., a very small spot size with high beam density and stability, determine the quality of the image obtained
We have developed an electrophoretic method of depositing a carbon nanotubes (CNTs) layer on the surface of a flat silicon cathode[20]
Its fabrication process follows the technology of miniature device under development, built from silicon electrodes and glass spacers
Summary
The electron beam parameters of an electron microscope, i.e., a very small spot size with high beam density and stability, determine the quality of the image obtained. These parameters depend on the electron gun. The choice of the electron gun is especially important in the realization of miniature electron-optical columns (microcolumns). Field cathodes are best suited for the fabrication of microcolumns due to their high brightness and small initial source size[1]. For SEM applications, RMS fluctuations of a few percent over 30 min at a relatively low angular emission current density of
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