Abstract
The technique of fast atom bombardment mass spectrometry has been applied to a range of mono- and poly-nuclear transition metal complexes which do not give electron impact mass spectra. In all cases the spectra are structurally informative, although not all show molecular ( M +) or quasi-molecular ([ M = H] +) ions. In the cases where no M + or [ M + H] + ions are observed, there appears to be a correlation between the ion of highes mass present and the known solution behaviour of the compound. In the case of the two cluster compounds both positive and negative ions are formed.
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