Abstract

The classical falling sphere method based onStokes' law is well known. Using gravitational forces, however, restricts the range of measurements considerably. This advantage can be overcome by applying iron spheres in a magnetic field, which allows to measure polymer melts with viscosities up to η0=109 Pa s (with very strong magnets available even more). A special measuring cell designed for application in the magnetic field is tested with several silicon oils in the gravitational field too. In both cases wall and end corrections toStokes' law have to be considered and are of main concern. Another important point is a reliable temperature measurement. Results especially for the high viscosity region of polymer melts are given.

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