Facile Synthesis of (E)-4-Aryl-2-Methyl-3-Butenoic Acids and Their Methyl Esters by the Condensation of Tiglic Acid Dianion with Arynes

Long Tran,Rakeb A Deshmukh,Ed Biehl

doi:10.1080/00397919608003700

Facile Synthesis of (E)-4-Aryl-2-Methyl-3-Butenoic Acids and Their Methyl Esters by the Condensation of Tiglic Acid Dianion with Arynes

Long Tran, Rakeb A Deshmukh + Show 1 more

https://doi.org/10.1080/00397919608003700

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Journal: Synthetic Communications	Publication Date: Mar 1, 1996
Citations: 5

Affiliation: Southern Methodist University

#Methyl Esters #Acid Dianion + Show 2 more

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Abstract

Abstract The condensation of various arynes with tiglic acid dianion yields (E)-4-aryl-2-methyl-3-butenoic acids exclusively, after proton quench. These acids were characterized as their methyl esters, which were prepared by treating the acids with diazomethane.

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