Abstract
In this work, we present an easy approach to prepare zirconium carbide (ZrC) nanofibers by electrospinning technique. Polyzirconoxane (PZO) is used as the zirconium source. Polyacrylonitrile (PAN) is used as the spinning aid and primary carbon source while sucrose is used as the additional carbon source. The as-spun green fibers are converted to ZrC nanofibers after carbothermal reduction at 1400°C. Core–shell structured nanofibers are obtained when using PAN only as the carbon source, while more homogeneous nanofibers which are composed of uniformly nano-sized ZrC crystals are obtained when using PAN and sucrose as the carbon source. The carbon source has a strong influence on the fiber morphology by affecting the kinetics of the carbothermal reduction reaction. The obtained ZrC fibers are characterized by XRD, SEM and TEM.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
