Abstract

This data article refers to the paper “Towards green analysis of virgin olive oil phenolic compounds: extraction by a natural deep eutectic solvent and direct spectrophotometric detection” [1]. A deep eutectic solvent (DES) based on lactic acid and glucose was used as green solvent for phenolic compounds. Eight standard phenolic compounds were solubilized in the DES. Then, a set of extra virgin olive oil (EVOO) samples (n=65) were submitted to liquid–liquid extraction by the DES. The standard solutions and the extracts were analyzed by UV spectrophotometry. This article reports the spectral data of both the standard solutions and the 65 extracts, as well as the total phenolic content of the corresponding oils, assessed by the Folin–Ciocalteu assay.

Highlights

  • University of Bari, Department of Soil, Plant and Food Sciences, Via Amendola 165/a, I-70126 Bari, Italy article info

  • This data article refers to the paper “Towards green analysis of virgin olive oil phenolic compounds: extraction by a natural deep eutectic solvent and direct spectrophotometric detection” [1]

  • A deep eutectic solvent (DES) based on lactic acid and glucose was used as green solvent for phenolic compounds

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Summary

Data accessibility

Excel files UV spectra: liquid–liquid extraction (or direct solubilisation for standard phenolic compounds) followed by UV absorption analysis (Agilent Cary 60 spectrophotometer, Agilent Technologies, Santa Clara, USA). Phenolic compounds content: liquid-liquid extraction followed by Folin-Ciocalteu assay Pre-processed Oil samples were directly submitted to liquid-liquid extraction. Water/methanol extracts were submitted to the Folin-Ciocalteu assay for determination of phenolic compounds content. DES extracts were submitted to direct UV absorption analysis Bari, Italy This data is available for spectrum processing UV spectra of some standard phenolic compounds solubilized in the DES under investigation are available for spectra comparisons and evaluation of spectroscopic properties of phenolic compounds. Supplementary material S1 reports the UV absorption spectra in the range 252–360 nm of 8 standard phenolic compounds – belonging to different chemical classes: benzoic acid derivatives (hydroxybenzoic acid, protocathecuic acid, vanillic acid), cinnamic acid derivatives (p-coumaric acid, caffeic acid), phenyl-ethyl alcohols (tyrosol), flavonoids (apigenin), lignans (pinoresinol) – after solubilization in the DES based on lactic acid and glucose. Mean spectra of the two independent extractions after sample weight normalization are reported

Reagents and samples
DES preparation
Extraction and determination of phenolic compounds
Extraction with DES
Findings
Acquisition of UV spectra of DES extracts
Full Text
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