Abstract

Process intensification during gas–liquid flows is of paramount importance to optimize the size of the chemical reactors. This paper results from an investigation of the mass transfer visualization in a millimetric tube by using the colorimetric technique. A slug bubble train has been established in a 3.8 mm diameter tube for different gas superficial velocities and a constant liquid superficial velocity resulting in the low capillary number range between 0.0004<Ca<0.0006. Color-inducing dye Resazurin solution interacts with the Oxygen bubble to induce the pink color in the solution which has been captured by a high-speed camera. The liquid slug entrapped between the bubbles has three distinct regions namely, the central stem which has a stagnation point ahead of the bubble, the wall lubrication layer, and an entrapped Taylor vortex between the central stem and wall lubrication layer. Flow visualization results have been correlated with the penetration theory-based mass transfer models.

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