Experimental study on small-scale hydrogen liquefaction of 0.5 L/h

Abstract

A small-scale hydrogen liquefaction device based on two-stage G-M refrigerator was designed and manufactured. Many practical operation processes on the liquefaction device were conducted in the open-air test base. The experimental results shown that 1) The direct liquefaction scheme of micro-positive pressure with normal temperature hydrogen realized by two-stage pressure reducing valve was feasible and effective; 2) Design of four-stage heat exchanger for G-M refrigerator cold head was reasonable and reliable; 3) The liquefaction rate in pure hydrogen was 0.47 L/h, and liquefaction pressure can maintain the range of about 120 kPa∼160 kPa; 4) After venting hydrogen-helium mixture, the liquefaction rate of hydrogen was 0.439 L/h again. In other words, the previously filled helium in the liquid hydrogen Dewar could be discharged through multiple venting method. The residue helium had little effect on the hydrogen liquefaction rate; 5) The scheme of simultaneous liquefaction and transmission was proved to be feasible; 6) Operation process experience and safety precautions on the hydrogen liquefaction were summarized. The testing results provided a technical support for design and operation of small-scale hydrogen liquefactions.