Experimental study of liquid vaporization in a fluidized bed

Abstract

AbstractLiquid injection into a gas–solid fluidized bed has been applied in various industries, such as coating and granulation processes in pharmaceutical and food industries, reactor cooling in polyolefin production, fluid catalytic cracking, and fluid coking in the petroleum industry. A new experimental method has been successfully developed to monitor the vaporization rate of a liquid injected into a fluidized bed. In addition, it can be used to determine the mass of liquid accumulated in the bed at a steady state. With this new method, measurements have identified three phenomena that may increase the amount of liquid accumulated at steady state in a fluidized bed. (1) Gas mixing affects vaporization when the bed temperature is lower than the liquid boiling point. In liquid‐rich regions of the bed, local vapour may build up, limiting the vaporization rate. Consequently, suitable emulsion to bubble gas transfer reduces the amount of accumulated liquid. (2) Solids mixing: hot particles from the rest of the bed must mix with the wetted particles to provide enough heat for vaporization. Good solids mixing reduces the amount of accumulated liquid. (3) Wet agglomerates formation: liquid trapped within wet agglomerates takes much longer to vaporize. The amount of accumulated liquid can be reduced by injecting the liquid in a well‐agitated bed region, operating at a higher bed temperature, or increasing the flowrate of atomization gas.