Experimental investigation on the influence of NaCl concentration on triaxial mechanical behaviors of a low-clay shale

Abstract

During a hydraulic fracturing operation, a large quantity of salinity fracturing fluids will be retained in the shale reservoir, which may cause the problem of wellbore instability. Previous studies mainly focused on the change mechanism of clay-rich shale after brine immersion. However, the influence of NaCl concentration on mechanical behaviors of a low-clay shale is still unclear. Therefore, in this investigation, conventional triaxial compression tests were carried out on low-clay shale specimens saturated with NaCl solutions at different concentrations (0%, 5%, 15%, 25%) under different confining pressures (0 MPa, 15 MPa, 30 MPa, 45 MPa), and their mechanical properties were analyzed systematically. Optical microscopy, polarized light microscopy and scanning electron microscopy were used to understand the microscopic changes in shale samples after saturation in NaCl solutions. The brittleness indices of saturated shale specimens were evaluated based on rock strength properties and the energy evolution law. According to the experimental results, compared with the water-saturated specimens, the peak strength, elastic modulus, cohesion and internal friction angle of specimens saturated with 5%NaCl solution all showed a downward trend. However, for the specimens saturated with the NaCl solution at concentrations of 15% and 25%, higher NaCl concentration showed a greater rebound effect on the mechanical parameters compared with the 5%NaCl saturation. The microscopic observation showed that the brine could invade the interior of shale specimens from micropores, microcracks and bedding fractures, which were mainly parallel to the bedding direction. And the bedding fractures and some of micropores seemed to be filled by deposited NaCl crystals and mineral particles. The brittleness index of the brine-saturated shale specimen decreased at the low-concentration (5%) and increased at the high-concentration (15% and 25%). This investigation could provide a theoretical basis and mechanical parameters for analyzing the stability of shale wellbore affected by the salinity fracturing fluids.