Experimental characterization and numerical analysis of CFRPs at cryogenic temperatures

Abstract

The thermo-mechanical performance of carbon fiber reinforced polymers (CFRPs) is affected by temperature changes due to the dissimilar nature of the constituents and dissimilar properties. For instance, under cryogenic conditions, the effective mechanical performance of the composite system can be significantly reduced. In this work, dynamic mechanical analysis (DMA) tests and coupon mechanical tests at room and cryogenic temperatures (through immersion in liquid nitrogen), are combined with computational micromechanics to analyze the development of micro-residual stresses from curing to cryogenic conditions, and their influence on the mechanical performance of a unidirectional CFRP. The results confirm the stiffness increase in the matrix and in the composite under cryogenic conditions, but the high tensile triaxial stress state that is developed during cooling reduces the overall composite strength, despite the increase of the matrix strength with decreasing temperature. To capture the failure modes and the evolution of the properties appropriately, the elastic-plastic response and the pressure dependent failure model are formulated to appropriately represent the shear response of the composite system and matrix failure under complex triaxial stress states, enabling a complete analysis and the identification of effective material properties, based on a reduced number of simple tests on the neat resin and on the composite system at different temperatures, which otherwise would be impossible to obtain considering the dimensional and technological restrictions of performing mechanical tests at cryogenic conditions.