Abstract
Pyranoid and furanoid spiro- N-mesyl azetidines, a new type of water-soluble spiro- C-nucleoside, have been prepared from easily available sugar spiroacetals (or glycosyl cyanides). The synthetic pathway involves opening of the acetalic ring with trimethylsilylcyanide, reduction, formation of an N, O-dimesylate, cyclization with sodium hydride in anhydrous DMF, and O-deprotection.
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