Abstract
In this study, evolution of phase and microstructure during synthesis of Ti(C,N) by carbothermal reduction–nitridation (CRN) of nanosized anatase/carbon black mixture were investigated using X‐ray diffraction (XRD) and scanning electron microscope (SEM). The results indicate phase evolution sequences are: TiO 2(anatase)→TiO 2(rutile)→Ti 5O 9→Ti 4O 7→Ti 3O 5→Ti(N,O)→TiN→Ti(C,N) or TiO 2 (anatase)→TiO 2 (rutile)→Ti 5O 9→Ti 4O 7→Ti 2O 3→Ti(C,N,O)→Ti(C,N). During initial stage of CRN reaction, the pronounced grain growth of the oxide particles was caused by the formation of lower titanium oxides. However, products grain was gradually diminished with the formation of cubic phase.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
