Abstract
Cyclopropenoids fatty acids (CPFA) from Sterculia striata seed oil were characterized by gas chromatography/mass spectrometry (GC/MS) and quantified by gas chromatography–flame ionization detector (GC–FID) after derivation to fatty acid methyl esters using a cold base-catalyzed procedure. 1H nuclear magnetic resonance (NMR) analysis were done in oil and fatty acid methyl esters derivatives to quantify CPFA and verify artifacts formation during the base-catalyzed reaction. Similar quantities of CPFA were found in S. striata and Sterculia foetida seed oils before and after a base-catalyzed methylation by NMR analysis, with no artifact formation. These results were compatible with those obtained by GC–FID analysis. Transmethylation with KOH in methanol was an appropriated method to prepare cyclopropenoids fatty acids methyl esters and quantify them by GC and NMR analysis.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
