Abstract

In the title compound, C28H26N4O4, the tetra­hydro­pyridine ring adopts a boat conformation. The two phenyl rings form dihedral angles of 88.64 (8) and 59.28 (10)° with the best plane through the tetra­hydro­pyridine ring. The dihedral angle between the two phenyl rings is 82.55 (10)°. The benzotriazole ring system is essentially planar, with a maximum deviation of 0.009 (1) Å from the least-squares plane. The mol­ecular conformation is stabilized by an intra­molecular O—H⋯O hydrogen bond, generating an S(6) motif.

Highlights

  • In the title compound, C28H26N4O4, the tetrahydropyridine ring adopts a boat conformation

  • The molecular conformation is stabilized by an intramolecular O—HÁ Á ÁO hydrogen bond, generating an S(6) motif

  • Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: BT5557)

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Summary

Structure Reports Online

C28H26N4O4, the tetrahydropyridine ring adopts a boat conformation. The two phenyl rings form dihedral angles of 88.64 (8) and 59.28 (10) with the best plane through the tetrahydropyridine ring. The dihedral angle between the two phenyl rings is 82.55 (10). The benzotriazole ring system is essentially planar, with a maximum deviation of 0.009 (1) Afrom the least-squares plane. The molecular conformation is stabilized by an intramolecular O—HÁ Á ÁO hydrogen bond, generating an S(6) motif. Related literature For the synthesis and medicinal properties of piperidin-4-onebased amides, see: Aridoss et al (2010a). For related structures see: Aridoss et al (2010a, 2010b, 2011). See: Cremer & Pople (1975); Nardelli (1983)

Bruker SMART APEXII areadetector diffractometer
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