Enhancing the applicability of near infrared spectroscopy for estimating specific gravity of green timber from Eucalyptus tereticornis by developing composite calibration using both radial and tangential face of wood

Abstract

Specific gravity is a very important factor in determining the economics of wood and wood products. This study is aimed to apply the near infrared spectroscopy technique with integrating sphere and fiber optic probe accessories for fast prediction of specific gravity of green timber (moisture content 27–30 %) of Eucalyptus tereticornis from 10 to 12 year old plantation. Specific gravity (basic density) was determined by conventional method (oven dry wt/green volume) and correlated with near infrared spectra using partial least square (PLS) regression. Calibrations using radial face, tangential face and composite face (both radial and tangential) were developed and compared. Coefficient of determination of cross validation (\( {\text{r}}_{\text{cv}}^{ 2} \)) for radial-longitudinal, tangential-longitudinal solid strips samples and composite face (both radial and tangential) was between 0.74–0.77 and 0.64–0.77 using integrating sphere and fiber optic probe, respectively. The coefficient of determination of prediction (\( {\text{r}}_{\text{p}}^{ 2} \)) was between 0.73–0.85 (with integrating sphere) and 0.69–0.83 (with fiber optic probe). The ratio of performance deviation (RPD) ranges from 2.06 to 2.46 for all models. Root mean square error of prediction (RMSEP) was higher than root mean square error of cross validation (RMSECV). For composite models with radial and tangential face \( {\text{r}}_{\text{cv}}^{ 2} \)/\( {\text{r}}_{\text{p}}^{ 2} \) was 0.74/0.76 using integrating sphere and 0.71/0.83 with fiber optic probe with Quant 2 automatic factors optimization process. The results indicate that the composite model is just as good as the radial and tangential face models and can adequately address the problem where it is difficult to obtain perfect radial or tangential surface, particularly in small girth plantation timber or where surface recognition is difficult.