Enhancing mechanical properties in Mg microtubes using tubular channel angular pressing-extrusion (TCAPE): A promising severe plastic deformation method

Abstract

In this study, a novel method, Tubular Channel Angular Pressing-Extrusion (TCAPE), is introduced for manufacturing ultrafine microtubes. This method, integrating Tubular Channel Angular Pressing (TCAP) and microtube extrusion (MTE) processes, reduces the number of stages in the fabrication of ultrafine microtubes while achieving favorable mechanical properties. In the TCAPE process, the tube undergoes Severe Plastic Deformation (SPD) in the shaping region and is subsequently shaped into the desired geometric dimensions through the extrusion process at the end. To investigate the effect of the number of SPD passes on the microstructure and mechanical properties of the produced microtubes, one-pass and two-pass SPD were applied. Metallography, XRD testing, tensile testing, and hardness measurement were employed for analysis. For a one-pass SPD, the sample was processed only through the TCAPE process (TCAP + MTE), while for a two-pass SPD, the sample underwent the TCAP process first and then underwent TCAPE for the second processing step (2TCAP + MTE). Tensile test results indicate an increase in Ultimate Tensile Strength (UTS) from the initial value of 73 MPa–103.1 MPa and 148 MPa, and elongation altered from the initial value of 10 to 7.1 and 17.5 after two-pass SPD. Metallography results show a reduction in grain size from the initial value of 160 μm to 15 μm and 3 μm after two-pass SPD. The TCAPE process, due to applying higher strain (1.955) compared to the TCAP process (1.64), exhibits better performance in refining the microstructure and improving mechanical properties. The hardness and ultimate strength of the TCAPE-processed sample are 13.33% and 13.5% higher than those of the TCAP-processed sample, respectively.