Abstract
A remarkable increase in the luminescent intensity of Er3+-doped CaF2 up-conversion phosphors was achieved, showing an approximate enhancement of over 1100-fold. This enhancement was realized by incorporating Yb3+, Al3+, Sr2+, and gold nanospheres and nanorods. The substantial improvement in up-converting luminescence effectively enhances sensitivity and efficiency at low excitation power densities. The up-conversion phosphors, consisting of (Ca,Sr)F2:Er,Yb,Al, were easily prepared using excess NH4F flux at 950 °C for 30 min. The structural confirmation of interstitial Al3+ ions within the CaF2 lattice was achieved through synchrotron powder X-ray powder diffraction. The significant enhancement of up-conversion emission and their mechanisms in the phosphors were vividly represented through energy transfer, interstitials and local distortions, and localized surface plasmon resonances when excited with a 980 nm diode laser.
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