Abstract

In the present work, duplex stainless steels (DSSs) SAF2507 were friction stir processed with flowing cryogenic medium mixed with liquid nitrogen and industrial ethanol. Homogeneous ultrafine grained (UFG) dual-phase structure with ferrite (α) and austenite (γ) grains with average size of around 1 μm was obtained due to the significantly lower peak temperature and shorter high-temperature duration. The developed UFG dual-phase structure enabled a dramatic enhancement of yield strength by about 22 %, while maintaining a high elongation of 55 % owing to the excellent strain hardening capacity. The grain refinement and increased number of α/γ interfaces were dominantly responsible for the significantly improved YS, while the massive development of geometrically necessary dislocations around the deformation incompatible α/γ interfaces primarily contributed to improving the strain hardening capacity. As a result, the enhanced strength-ductility synergy was achieved by cryogenic friction stir processing. Also, the obtained UFG dual-phase structure helps with enhancing corrosion resistance. This work provides a new strategy for preparing uniform UFG DSSs with outstanding mechanical properties and anticorrosion.

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