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Abstract
Simultaneous enhancement of the strength and ductility in metal-matrix nanocomposites with high content nano-reinforcements is crucial for the development of novel composite materials. Here SiC/Al nanocomposites with ultrafine Al grains and intragranular 10 vol% SiC nanoparticle were prepared by mechanical alloying and hot pressure sintering followed by hot extrusion. The results show that nanocrystalline Al grains and uniformly distributed SiC nanoparticles (SiCnp) in the composite powders are obtained after ball-milling. The prior particle boundary (PPB) in the composite powders cannot be fully removed by sintering at 580 °C under 20 MPa, but can be eliminated by subsequent hot extrusion at 450 °C with a ratio 25:1. The extruded nanocomposites possess ultrafine Al grains with diameter 320 nm and intragranular SiCnp created by the dynamic recrystallizations (DRX). Such optimal microstructure favors a significant improvement of 284% in yield strength (YS) and 259% in ultimate tensile strength (UTS) compared with monolithic Al, and more interestingly, maintains an elongation up to 12% due to the homogeneous nanoparticles in fine Al grains. Theoretical analysis shows that the dominant strengthening factor is Orowan strengthening related to the high content intragranular SiCnp, with second factor grain boundary strengthening due to ultrafine Al grains.
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