Abstract
The enantiospecific synthesis of the diacid side-chain of deoxyharringtonine (2) and homodeoxyharringtonine (3) was accomplished from (L)-N-Boc-α-amino alcohol 10 in high yield. A key feature of the synthesis is the construction of the chiral tertiary alcohol by a three-step sequence (i.e., Wittig reaction, Meisenheimer rearrangement, and catalytic hydrogenation).
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