Abstract

Emanation Thermal Analysis (ETA) was used to characterize microstructure changes of hydrous ruthenia and hydrous ruthenia-titania as precursors for preparation of RuO2 and (RuO2)0.9-(TiO2)0.l by heating in the temperature range of 20–600°C in argon. A good agreement was found between ETA, TG and DTA results, X-ray diffraction patterns and surface area measurements of intermediate products of the thermal treatment.

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