Abstract

Elevated temperature compression testing has been conducted in air at 1200 and 1300K with strain rates varying from ∼10−4 to ∼10−7sec−1 on NiAl-TiB2 particulate composites. These materials, which consisted of a B2 crystal structure intermetallic Ni-50at% Al matrix and from 0 to 30 vol % of approximately 1 μm diameter TiB2 particles, were fabricated by XD synthesis and hot pressed to full density. Flow strength of the composites increased with volume fraction of the strengthening phase with NiAl-30TiB2 being approximately three times stronger than NiAl. Comparison of the light optical and transmission electron microstructures of asreceived and tested samples revealed that reactions did not occur between the two phases, and NiAl-TiB2 interfaces were not cracked during deformation. Additional transmission electron microscopy indicated that the particles stabilize a vastly different microstructure in the NiAl matrix of the composites than that formed in unreinforced NiAl.

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