Abstract
Following known procedures for the preparation of nickel complexes as precursors to active contact species for the cyclooligomerization of acetylene we report the electrochemical formation of Ni(CO)2(PPh3)2 and its use in a one-pot trimerization of acetylene to benzene. Further investigations demonstrate the possibility to simultaneously produce and use as catalysts active nickel solvates generated from nickel anodes for the cyclization of acetylene to benzene and/or cyclooctatetraene.
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