Abstract
AbstractElectrochemical Synthesis of Ag5Pb2O6Ag5Pb2O6 was prepared by anodic oxidation of silver in a PbO2 suspension in an aqueous KOH solution. Phase purity was checked by a Rietveld‐fit of the X‐ray powder pattern, thermal and chemical analysis. The compound exhibits ionic conductivity. It' anisotropy leads to an orientation of the crystallites on the silver anode.
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