Abstract
Abstract Synthetic photoelectrochemistry (PEC), the fusion of photoredox catalysis (PRC), and synthetic organic electrochemistry (SOE) provide a powerful way for the selective C(sp 2 )/C(sp 3 )H functionalization via single‐electron transfer (SET). Compared with PRC and SOE, PEC shows stronger redox ability under mild conditions and significant atomic and energy economy. The combination of PEC with hydrogen atom transfer (HAT) makes the inert CH activation possible. Herein, the corresponding work is reviewed by the classification of the formation of CO, CC, CN, and CP bonds.
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