Abstract

Five iodinating reagents were compared to determine the percentage iodination of benzene under similar conditions. Both ICI and chloramine-T in a 1:1 mixture of trifluoroacetic acid and trifluoroacetic anhydride gave high iodination yields using 0.2 M benzene as substrate. Chloramine-T in a 1:1 mixture of trifluoroacetic acid and trifluoroacetic acid anhydride is the system of choice of those studied for no-carrier-added iodination.

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