Abstract
Whereas compounds containing unactivated double bonds generally react with trifluoro(fluoro-oxy)methane to afford complex mixtures of products, allylic alcohols and acetates each give cleanly two adducts which correspond to the cis-addition of CF3OF and of F2. Evidence is presented that the orientation of the allylic oxygen function is not important and that intramolecular nucleophilic participation is not involved.
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