Abstract
The single NO bond in various ethers derived from 1-hydroxybenzo( d)-1,2,3-triazoles is reduced at mercury cathodes in a 2-electron process giving rise to the non-substituted benzotriazole and a corresponding primary alcohol. Controlled-potential electrolysis actually resulted in isolating the products of the above type eg benzotriazole and 2-piperidinoethanol. Cathodic reduction of non-substituted benzotriazole in acid media proceeds evidently via a chemical reaction between benzotriazole and hydrogen obtained by the catalytic reduction of hydrogen ions at the mercury electrode.
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