Abstract
Two chronopotentiometric waves were observed for the electrochemical reduction of molybdate in the presence of zinc chloride, with quarter‐wave potentials of −1.5V and −1.75V vs. the Pt(II)/Pt reference electrode, respectively. It was observed that an increase in the molybdate concentration causes a decrease of the first transition time indicating a chemical reaction between (which is reduced at −1.5V) and in the melt forming which is sparingly dissociated in eutectic. The equilibrium constant for the observed reaction was calculated. X‐ray powder diffraction patterns of the reduction product of have been obtained.
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