Abstract
Bismuth(III) alkoxides have been synthesized by electrochemical reactions of methanol, ethanol, n-propanol, n-butanol, n-pentanol, n-hexanol, n-heptanol, n-octanol, n-onanol, n-decanol at sacrificial bismuth anode and inert platinum cathode using tetrabutylammonium chloride as supporting electrolyte and acetonitrile as solvent. The solid products separated in the anode compartment have been isolated and characterized by elemental analysis and infrared spectral studies. Current efficiencies of these reactions are quite high.
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