Abstract
Summary of main observation and conclusionTetrasubstituted olefins are significant scaffolds as they are prevalent in many biologically active compounds and versatile building blocks for organic synthesis. Herein, we report an electrochemical oxidative Csp3—H/S—H cross‐coupling reaction, in which various tetrasubstituted olefins were prepared under base‐free, transition metal‐free, and oxidants‐free reaction conditions.
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