Abstract
The electrochemical oxidation of a cyclic peralkylsilane derivative,[( n-Pr) 2Si] 5 (I), in dichloromethane in the presence of ClO 4 − or AcO − salts, leads to both oxygen insertion and ring-opening processes, to form mainly cyclic and linear siloxanes. The latter contain various groups at their terminal positions: OH, AcO, CH 2CN or n-propyl.
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