Abstract
Abstract Hydrogen production and CO2 energy conversion have increasingly attracted attention and developing electrochemical energy catalysts has widely been performed to achieve clean energy and energy-recycle goals. Herein, hierarchical MoSxSe2-x hybrid nanostructures were synthesized by the hydrothermal method, and the fundamental physiochemical properties were fully characterized by X-ray diffraction crystallography, scanning electron microscopy, high-resolution transmission electron microscopy, elemental mapping, Raman, and X-ray photoelectron spectroscopy. Electrochemical hydrogen evolution reaction was tested in an acidic electrolyte to show a catalytic activity order of MoS2
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