Abstract

Abstract Spin adduct aminoxyls (nitroxides) produced from the reaction of shortlived radicals with α-phenyl-tert-butyl nitrone (PBN) could be separated by high performance liquid chromatography (HPLC) and analyzed by both UV and electrochemical detectors. Peak assignments of the spin adduct aminoxyls were confirmed by collecting peak effluents and analyzing by electron spin resonance (ESR) spectroscopy. Mixtures of aminoxyl spin adducts that were unresolvable by ESR methods were separated by HPLC and their individual ESR spectra recorded.

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.