Abstract
A constant current electrolysis of saturated aliphatic ketones in a CH3CN or DMF solution containing 0.1 mol dm−3 Bu4NBF4 with a platinum cathode and a magnesium anode under an atmospheric pressure of CO2 resulted in an efficient fixation of CO2 at α-position of carbonyl group in the ketones to give the corresponding β-keto carboxylic acids in moderate to good yields.
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